TA Instruments

AR1771-0001f

28/03/2013 11:13:10

Sample name	DI 40 mm AL P240B 10 mm gap
Sample notes	 
Experiment notes	DI Deionised water, 40 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	mr1
Sample density	1.000 g/cm^3
Results file name	AR1771
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	28/03/2013 11:13:10

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	40 mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	40.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	2.000 
Shear stress factor	79580 1/m^3
Measurement system factor	39790 1/m^3
Fluid density factor	8.378E-10 m^5
Normal force factor	1592 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	12.57 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	5.966	-39.183	10000	20.0	5.878	31.004	-3.118	11.93	-0.2613	9355	5.3521	65.71	10.704	1070.4	3.411E-3	0.0	0.5
1.9960	9.801	12.084	10000	20.0	5.876	31.996	0.9616	19.60	0.04906	9352	13.1766	24.34	26.353	2635.3	3.411E-3	0.0	0.5
3.0000	15.47	23.264	10000	20.0	5.876	33.000	1.851	30.93	0.05985	9352	26.9252	9.773	53.850	5385.0	3.411E-3	0.1	0.6
3.9960	18.41	30.325	10000	20.0	5.876	33.996	2.413	36.81	0.06555	9351	40.7925	6.900	81.585	8158.5	3.411E-3	0.1	0.6
4.9960	24.66	46.906	10000	20.0	5.871	34.996	3.733	49.32	0.07568	9345	67.6299	3.842	135.26	13526	3.411E-3	0.1	0.6
6.0040	31.57	68.982	10000	20.0	5.872	36.004	5.489	63.14	0.08694	9346	106.6060	2.344	213.21	21321	3.411E-3	0.1	0.6
7.0000	34.01	76.926	10000	20.0	5.871	37.000	6.122	68.03	0.08999	9344	126.4070	2.019	252.81	25281	3.411E-3	0.1	0.6
7.9960	39.29	95.993	10000	20.0	5.867	37.996	7.639	78.58	0.09721	9337	165.3430	1.512	330.69	33069	3.411E-3	0.1	0.6
8.9960	46.02	123.54	10000	20.0	5.862	38.996	9.831	92.04	0.1068	9329	223.0630	1.101	446.13	44613	3.411E-3	0.1	0.6
9.9920	50.95	145.12	10000	20.0	5.860	39.992	11.55	101.9	0.1133	9327	274.9340	0.8983	549.87	54987	3.411E-3	0.2	0.7
11.004	55.71	166.91	10000	20.0	5.852	41.004	13.28	111.4	0.1192	9314	325.9960	0.7502	651.99	65199	3.411E-3	0.2	0.7
11.996	60.09	189.63	10000	20.0	5.850	41.996	15.09	120.2	0.1256	9311	377.0880	0.6447	754.18	75418	3.411E-3	0.2	0.7
12.996	64.40	212.26	10000	20.0	5.847	42.996	16.89	128.8	0.1311	9306	435.6300	0.5610	871.26	87126	3.411E-3	0.2	0.7
13.996	69.13	237.46	10000	20.0	5.844	43.996	18.90	138.3	0.1367	9301	498.7970	0.4865	997.59	99760	3.411E-3	0.2	0.7
15.000	75.67	274.58	10000	20.0	5.836	45.000	21.85	151.3	0.1444	9289	594.0090	0.4056	1188.0	1.1880E5	3.411E-3	0.3	0.8
16.012	79.92	300.25	10000	20.0	5.833	46.012	23.89	159.8	0.1495	9283	664.0200	0.3634	1328.0	1.3280E5	3.411E-3	0.3	0.8
17.008	84.52	327.83	10000	20.0	5.826	47.008	26.09	169.0	0.1543	9272	740.4460	0.3245	1480.9	1.4809E5	3.411E-3	0.3	0.8
18.004	90.97	368.81	10000	20.0	5.813	48.004	29.35	181.9	0.1613	9252	855.1760	0.2795	1710.4	1.7104E5	3.411E-3	0.3	0.8
19.008	95.03	391.33	10000	20.0	5.812	49.008	31.14	190.1	0.1639	9251	931.0100	0.2561	1862.0	1.8620E5	3.411E-3	0.3	0.8
20.012	99.39	425.65	10000	20.0	5.805	50.012	33.87	198.8	0.1704	9239	1019.8900	0.2338	2039.8	2.0398E5	3.411E-3	0.3	0.8
21.004	105.8	467.49	10000	20.0	5.792	51.004	37.20	211.6	0.1758	9218	1153.1200	0.2058	2306.2	2.3062E5	3.411E-3	0.4	0.9
22.012	109.9	495.89	10000	20.0	5.781	52.012	39.46	219.8	0.1795	9200	1243.5500	0.1905	2487.1	2.4871E5	3.411E-3	0.4	0.9
23.000	114.2	530.76	10000	20.0	5.778	53.000	42.24	228.5	0.1849	9195	1343.2500	0.1762	2686.5	2.6865E5	3.411E-3	0.4	0.9
24.012	120.6	577.78	10000	20.0	5.765	54.012	45.98	241.3	0.1906	9175	1495.3700	0.1576	2990.7	2.9907E5	3.411E-3	0.4	0.9
25.012	124.7	602.81	10000	20.0	5.761	55.012	47.97	249.5	0.1923	9169	1597.5900	0.1474	3195.2	3.1952E5	3.411E-3	0.4	0.9
25.996	129.1	639.19	10000	20.0	5.752	55.996	50.87	258.1	0.1971	9154	1710.7000	0.1374	3421.4	3.4214E5	3.411E-3	0.4	0.9
26.996	135.4	693.16	10000	20.0	5.743	56.996	55.16	270.9	0.2036	9141	1882.7200	0.1246	3765.4	3.7654E5	3.411E-3	0.4	0.9
27.996	139.5	732.68	10000	20.0	5.733	57.996	58.30	279.1	0.2089	9125	1995.4200	0.1172	3990.8	3.9908E5	3.411E-3	0.5	1.0
29.012	143.6	763.38	10000	20.0	5.726	59.012	60.75	287.3	0.2115	9113	2116.3201	0.1104	4232.6	4.2326E5	3.411E-3	0.5	1.0
29.996	150.0	822.59	10000	20.0	5.719	59.996	65.46	300.1	0.2182	9102	2305.3201	0.1011	4610.6	4.6106E5	3.411E-3	0.5	1.0
31.020	154.2	852.04	10000	20.0	5.705	61.020	67.80	308.3	0.2199	9080	2431.8999	0.09552	4863.8	4.8638E5	3.411E-3	0.5	1.0
31.996	158.2	894.69	10000	20.0	5.702	61.996	71.20	316.5	0.2250	9074	2565.3999	0.09059	5130.8	5.1308E5	3.411E-3	0.5	1.0
33.004	164.6	950.87	10000	20.0	5.689	63.004	75.67	329.3	0.2298	9054	2773.1399	0.08350	5546.3	5.5463E5	3.411E-3	0.6	1.1
34.012	168.8	995.10	10000	20.0	5.674	64.012	79.19	337.5	0.2346	9030	2912.1599	0.07926	5824.3	5.8243E5	3.411E-3	0.6	1.1
35.012	174.9	1051.9	10000	20.0	5.665	65.012	83.71	349.7	0.2393	9016	3127.0601	0.07372	6254.1	6.2541E5	3.411E-3	0.6	1.1
36.000	179.1	1090.3	10000	20.0	5.663	66.000	86.76	358.2	0.2422	9013	3278.6001	0.07024	6557.2	6.5572E5	3.411E-3	0.6	1.1
36.996	183.2	1133.9	10000	20.0	5.647	66.996	90.23	366.5	0.2462	8987	3430.3501	0.06691	6860.7	6.8607E5	3.411E-3	0.6	1.1
38.008	189.3	1198.0	10000	20.0	5.631	68.008	95.34	378.6	0.2518	8961	3657.8201	0.06253	7315.6	7.3156E5	3.411E-3	0.6	1.1
38.996	193.5	1246.4	10000	20.0	5.622	68.996	99.18	386.9	0.2563	8948	3822.5500	0.05977	7645.1	7.6451E5	3.411E-3	0.6	1.1
40.012	199.7	1296.5	10000	20.0	5.614	70.012	103.2	399.3	0.2584	8935	4069.1699	0.05603	8138.3	8.1383E5	3.411E-3	0.7	1.2
41.012	203.7	1366.7	10000	20.0	5.597	71.012	108.8	407.3	0.2670	8907	4232.2598	0.05368	8464.5	8.4645E5	3.411E-3	0.7	1.2
41.992	207.9	1400.3	10000	20.0	5.582	71.992	111.4	415.7	0.2680	8884	4409.9902	0.05140	8820.0	8.8200E5	3.411E-3	0.7	1.2
43.008	214.1	1468.1	10000	20.0	5.574	73.008	116.8	428.1	0.2729	8871	4674.0898	0.04839	9348.2	9.3482E5	3.411E-3	0.7	1.2
43.996	218.1	1527.5	10000	20.0	5.557	73.996	121.6	436.2	0.2787	8845	4851.6699	0.04648	9703.3	9.7033E5	3.411E-3	0.7	1.2
44.996	224.3	1590.8	10000	20.0	5.549	74.996	126.6	448.5	0.2822	8831	5134.9600	0.04390	10270	1.0270E6	3.411E-3	0.7	1.2
46.000	228.4	1638.7	10000	20.0	5.532	76.000	130.4	456.8	0.2855	8804	5317.6899	0.04219	10635	1.0635E6	3.411E-3	0.8	1.3
47.012	234.5	1704.0	10000	20.0	5.505	77.012	135.6	469.0	0.2891	8762	5603.4502	0.03984	11207	1.1207E6	3.411E-3	0.8	1.3
48.012	238.5	1757.5	10000	20.0	5.498	78.012	139.9	477.0	0.2932	8750	5797.0898	0.03845	11594	1.1594E6	3.411E-3	0.8	1.3
49.012	242.7	1802.6	10000	20.0	5.491	79.012	143.4	485.3	0.2956	8739	5999.1699	0.03710	11998	1.1998E6	3.411E-3	0.8	1.3
50.000	248.8	1893.8	10000	20.0	5.476	80.000	150.7	497.5	0.3029	8715	6301.8398	0.03521	12604	1.2604E6	3.411E-3	0.8	1.3
51.004	252.8	1955.5	10000	20.0	5.449	81.004	155.6	505.6	0.3078	8672	6509.7998	0.03392	13020	1.3020E6	3.411E-3	0.9	1.4
51.996	259.0	2026.6	10000	20.0	5.424	81.996	161.3	518.1	0.3113	8632	6831.5698	0.03216	13663	1.3663E6	3.411E-3	0.9	1.4
52.996	263.1	2094.6	10000	20.0	5.417	82.996	166.7	526.1	0.3168	8621	7046.1001	0.03114	14092	1.4092E6	3.411E-3	0.9	1.4
54.012	269.1	2194.6	10000	20.0	5.391	84.012	174.6	538.3	0.3244	8580	7373.8398	0.02961	14748	1.4748E6	3.411E-3	0.9	1.4
55.012	273.2	2259.7	10000	20.0	5.380	85.012	179.8	546.5	0.3290	8563	7600.8799	0.02867	15202	1.5202E6	3.411E-3	0.9	1.4
56.008	277.3	2323.5	10000	20.0	5.349	86.008	184.9	554.7	0.3333	8514	7828.0098	0.02767	15656	1.5656E6	3.411E-3	0.9	1.4
56.996	283.4	2442.2	10000	20.0	5.310	86.996	194.3	566.7	0.3429	8451	8173.7100	0.02631	16347	1.6347E6	3.411E-3	0.9	1.4
58.012	287.4	2532.7	10000	20.0	5.298	88.012	201.5	574.9	0.3506	8432	8408.2197	0.02551	16816	1.6816E6	3.411E-3	1.0	1.5
59.012	293.6	2648.4	10000	20.0	5.258	89.012	210.7	587.1	0.3589	8369	8770.2803	0.02428	17541	1.7541E6	3.411E-3	1.0	1.5
60.012	297.6	2759.1	10000	20.0	5.241	90.012	219.6	595.2	0.3689	8342	9008.4102	0.02355	18017	1.8017E6	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	300.0	2792.9	10000	20.0	5.228	92.004	222.2	600.0	0.3704	8320	305.2540	0.02311	610.51	61051	3.411E-3	0.0	1.5
2.0160	300.0	2778.0	10000	20.0	5.206	93.016	221.1	600.0	0.3684	8286	555.9090	0.02302	1111.8	1.1118E5	3.411E-3	0.0	1.6
3.0120	300.0	2771.4	10000	20.0	5.215	94.012	220.5	600.0	0.3676	8300	807.2780	0.02306	1614.6	1.6146E5	3.411E-3	0.1	1.6
4.0080	300.0	2801.4	10000	20.0	5.217	95.008	222.9	600.0	0.3716	8302	1183.0300	0.02307	2366.1	2.3661E5	3.411E-3	0.1	1.6
5.0160	300.0	2857.5	10000	20.0	5.204	96.016	227.4	600.0	0.3790	8283	1434.4200	0.02301	2868.8	2.8688E5	3.411E-3	0.1	1.6
6.0200	300.0	2837.7	10000	20.0	5.199	97.020	225.8	600.0	0.3763	8275	1813.0400	0.02299	3626.1	3.6261E5	3.411E-3	0.1	1.6
7.0160	300.0	2855.1	10000	20.0	5.210	98.016	227.2	600.0	0.3787	8291	2066.7000	0.02303	4133.4	4.1334E5	3.411E-3	0.1	1.6
8.0000	300.0	2802.9	10000	20.0	5.204	99.000	223.1	600.0	0.3717	8282	2314.1299	0.02300	4628.3	4.6283E5	3.411E-3	0.1	1.7
9.0080	300.0	2815.9	10000	20.0	5.208	100.008	224.1	599.9	0.3735	8288	2691.2300	0.02303	5382.5	5.3825E5	3.411E-3	0.2	1.7
10.016	300.0	2860.8	10000	20.0	5.208	101.016	227.7	600.0	0.3794	8288	2942.4800	0.02302	5885.0	5.8850E5	3.411E-3	0.2	1.7
11.000	300.0	2806.0	10000	20.0	5.214	102.000	223.3	600.0	0.3722	8298	3321.9900	0.02305	6644.0	6.6440E5	3.411E-3	0.2	1.7
12.000	300.0	2832.9	10000	20.0	5.188	103.000	225.4	600.0	0.3757	8256	3572.8101	0.02293	7145.6	7.1456E5	3.411E-3	0.2	1.7
13.016	300.0	2857.2	10000	20.0	5.192	104.016	227.4	600.0	0.3790	8263	3822.1001	0.02295	7644.2	7.6442E5	3.411E-3	0.2	1.7
14.016	300.0	2870.7	10000	20.0	5.225	105.016	228.4	600.0	0.3807	8316	4199.1802	0.02310	8398.4	8.3984E5	3.411E-3	0.2	1.8
15.012	300.0	2804.3	10000	20.0	5.198	106.012	223.2	600.0	0.3719	8272	4450.6499	0.02298	8901.3	8.9013E5	3.411E-3	0.3	1.8
16.000	300.0	2824.7	10000	20.0	5.202	107.000	224.8	600.0	0.3746	8279	4701.8301	0.02300	9403.7	9.4037E5	3.411E-3	0.3	1.8
17.016	300.0	2806.6	10000	20.0	5.196	108.016	223.3	599.9	0.3723	8270	5078.9199	0.02298	10158	1.0158E6	3.411E-3	0.3	1.8
18.016	300.0	2814.0	10000	20.0	5.205	109.016	223.9	600.0	0.3732	8285	5331.7202	0.02301	10663	1.0663E6	3.411E-3	0.3	1.8
19.008	300.0	2807.4	10000	20.0	5.212	110.008	223.4	599.9	0.3724	8296	5707.2998	0.02305	11415	1.1415E6	3.411E-3	0.3	1.8
20.000	300.0	2819.0	10000	20.0	5.198	111.000	224.3	600.0	0.3739	8273	5959.2598	0.02298	11919	1.1919E6	3.411E-3	0.3	1.9
20.996	300.0	2818.1	10000	20.0	5.216	111.996	224.3	600.0	0.3738	8301	6210.9399	0.02306	12422	1.2422E6	3.411E-3	0.3	1.9
22.016	300.0	2822.4	10000	20.0	5.207	113.016	224.6	599.9	0.3744	8287	6586.5801	0.02302	13173	1.3173E6	3.411E-3	0.4	1.9
23.000	300.0	2845.8	10000	20.0	5.205	114.000	226.5	600.0	0.3774	8285	6838.1401	0.02301	13676	1.3676E6	3.411E-3	0.4	1.9
24.016	300.0	2825.1	10000	20.0	5.220	115.016	224.8	600.0	0.3747	8307	7214.9302	0.02307	14430	1.4430E6	3.411E-3	0.4	1.9
25.016	300.0	2790.6	10000	20.0	5.214	116.016	222.1	600.0	0.3701	8298	7466.2998	0.02305	14933	1.4933E6	3.411E-3	0.4	1.9
26.000	300.0	2812.4	10000	20.0	5.237	117.000	223.8	600.1	0.3730	8335	7717.8198	0.02315	15436	1.5436E6	3.411E-3	0.4	2.0
27.000	300.0	2803.1	10000	20.0	5.215	118.000	223.1	600.0	0.3718	8299	8097.0801	0.02305	16194	1.6194E6	3.411E-3	0.5	2.0
28.000	300.0	2829.8	10000	20.0	5.210	119.000	225.2	600.0	0.3753	8291	8346.4805	0.02303	16693	1.6693E6	3.411E-3	0.5	2.0
29.008	300.0	2813.0	10000	20.0	5.201	120.008	223.8	600.0	0.3731	8277	8725.5898	0.02299	17451	1.7451E6	3.411E-3	0.5	2.0
30.012	300.0	2822.5	10000	20.0	5.207	121.012	224.6	600.0	0.3743	8288	8974.2305	0.02302	17948	1.7948E6	3.411E-3	0.5	2.0
31.000	300.0	2816.0	10000	20.0	5.203	122.000	224.1	600.0	0.3735	8281	9225.7402	0.02300	18451	1.8451E6	3.411E-3	0.5	2.0
32.016	300.0	2819.1	10000	20.0	5.214	123.016	224.3	600.0	0.3739	8298	9602.5703	0.02305	19205	1.9205E6	3.411E-3	0.5	2.1
33.016	300.0	2834.2	10000	20.0	5.224	124.016	225.5	600.1	0.3759	8314	9853.9502	0.02309	19708	1.9708E6	3.411E-3	0.6	2.1
34.016	300.0	2861.4	10000	20.0	5.209	125.016	227.7	600.0	0.3795	8291	10108.300	0.02303	20217	2.0217E6	3.411E-3	0.6	2.1
35.016	300.0	2830.6	10000	20.0	5.191	126.016	225.2	600.0	0.3754	8261	10482.300	0.02295	20965	2.0965E6	3.411E-3	0.6	2.1
36.012	300.0	2866.9	10000	20.0	5.192	127.012	228.1	600.0	0.3802	8264	10733.700	0.02295	21467	2.1467E6	3.411E-3	0.6	2.1
37.016	300.0	2872.4	10000	20.0	5.206	128.016	228.6	600.0	0.3810	8286	11110.700	0.02302	22221	2.2221E6	3.411E-3	0.6	2.1
38.016	300.0	2799.6	10000	20.0	5.214	129.016	222.8	600.1	0.3713	8298	11362.100	0.02304	22724	2.2724E6	3.411E-3	0.6	2.2
39.016	300.0	2799.1	10000	20.0	5.222	130.016	222.7	600.0	0.3712	8311	11613.300	0.02308	23227	2.3227E6	3.411E-3	0.7	2.2
40.016	300.0	2835.7	10000	20.0	5.197	131.016	225.7	600.0	0.3761	8271	11991.100	0.02298	23982	2.3982E6	3.411E-3	0.7	2.2
41.016	300.0	2781.8	10000	20.0	5.215	132.016	221.4	600.1	0.3689	8299	12241.700	0.02305	24483	2.4483E6	3.411E-3	0.7	2.2
42.016	300.0	2840.2	10000	20.0	5.193	133.016	226.0	600.0	0.3767	8264	12620.100	0.02296	25240	2.5240E6	3.411E-3	0.7	2.2
43.016	300.0	2873.6	10000	20.0	5.199	134.016	228.7	600.0	0.3811	8274	12870.000	0.02298	25740	2.5740E6	3.411E-3	0.7	2.2
44.016	300.0	2862.1	10000	20.0	5.222	135.016	227.8	600.0	0.3796	8310	13122.300	0.02308	26245	2.6245E6	3.411E-3	0.7	2.3
45.016	300.0	2814.3	10000	20.0	5.195	136.016	224.0	600.1	0.3732	8268	13498.400	0.02296	26997	2.6997E6	3.411E-3	0.8	2.3
46.016	300.0	2809.1	10000	20.0	5.199	137.016	223.5	600.0	0.3726	8275	13749.600	0.02299	27499	2.7499E6	3.411E-3	0.8	2.3
47.000	300.0	2818.8	10000	20.0	5.192	138.000	224.3	600.0	0.3738	8263	14000.900	0.02295	28002	2.8002E6	3.411E-3	0.8	2.3
48.000	300.0	2826.4	10000	20.0	5.190	139.000	224.9	600.0	0.3748	8260	14377.900	0.02294	28756	2.8756E6	3.411E-3	0.8	2.3
49.020	300.0	2863.5	10000	20.0	5.193	140.020	227.9	600.0	0.3798	8265	14629.400	0.02296	29259	2.9259E6	3.411E-3	0.8	2.3
49.996	300.0	2878.0	10000	20.0	5.181	140.996	229.0	599.9	0.3818	8247	15007.400	0.02291	30015	3.0015E6	3.411E-3	0.8	2.3
51.024	300.0	2926.6	10000	20.0	5.177	142.024	232.9	600.0	0.3882	8240	15257.800	0.02289	30516	3.0516E6	3.411E-3	0.9	2.4
52.016	300.0	2802.4	10000	20.0	5.201	143.016	223.0	600.1	0.3716	8278	15508.800	0.02299	31018	3.1018E6	3.411E-3	0.9	2.4
53.016	300.0	2835.2	10000	20.0	5.210	144.016	225.6	600.0	0.3760	8292	15886.000	0.02303	31772	3.1772E6	3.411E-3	0.9	2.4
54.016	300.0	2848.5	10000	20.0	5.211	145.016	226.7	600.0	0.3778	8294	16137.200	0.02304	32274	3.2274E6	3.411E-3	0.9	2.4
55.000	300.0	2895.0	10000	20.0	5.190	146.000	230.4	600.0	0.3840	8260	16515.600	0.02295	33031	3.3031E6	3.411E-3	0.9	2.4
56.000	300.0	2850.5	10000	20.0	5.192	147.000	226.8	600.0	0.3781	8263	16767.199	0.02295	33534	3.3534E6	3.411E-3	0.9	2.5
57.016	300.0	2899.4	10000	20.0	5.206	148.016	230.7	599.9	0.3846	8285	17016.900	0.02302	34034	3.4034E6	3.411E-3	1.0	2.5
58.016	300.0	2884.0	10000	20.0	5.178	149.016	229.5	600.0	0.3825	8240	17395.000	0.02289	34790	3.4790E6	3.411E-3	1.0	2.5
59.012	300.0	2822.6	10000	20.0	5.198	150.012	224.6	600.0	0.3743	8274	17645.100	0.02298	35290	3.5290E6	3.411E-3	1.0	2.5
59.996	300.0	2856.4	10000	20.0	5.193	150.996	227.3	600.0	0.3789	8265	17896.500	0.02296	35793	3.5793E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0080	297.5	2838.4	10000	20.0	5.211	152.008	225.9	595.0	0.3796	8294	230.1810	0.02343	460.36	46036	3.411E-3	0.0	2.5
2.0040	291.5	2694.7	10000	20.0	5.236	153.004	214.4	583.0	0.3678	8333	586.9300	0.02452	1173.9	1.1739E5	3.411E-3	0.0	2.6
3.0080	287.5	2548.8	10000	20.0	5.277	154.008	202.8	574.9	0.3528	8398	825.0670	0.02541	1650.1	1.6501E5	3.411E-3	0.1	2.6
4.0120	281.3	2426.6	10000	20.0	5.334	155.012	193.1	562.6	0.3432	8489	1176.7000	0.02682	2353.4	2.3534E5	3.411E-3	0.1	2.6
5.0200	277.3	2335.1	10000	20.0	5.350	156.020	185.8	554.6	0.3351	8515	1401.1200	0.02768	2802.2	2.8022E5	3.411E-3	0.1	2.6
6.0080	273.2	2259.1	10000	20.0	5.353	157.008	179.8	546.5	0.3290	8520	1628.4100	0.02853	3256.8	3.2568E5	3.411E-3	0.1	2.6
7.0080	267.0	2166.2	10000	20.0	5.386	158.008	172.4	534.1	0.3227	8571	1964.7300	0.03005	3929.5	3.9295E5	3.411E-3	0.1	2.6
8.0200	263.0	2076.5	10000	20.0	5.413	159.020	165.2	526.0	0.3141	8615	2177.6299	0.03113	4355.3	4.3553E5	3.411E-3	0.1	2.7
9.0040	256.9	2006.7	10000	20.0	5.441	160.004	159.7	513.9	0.3107	8660	2497.8799	0.03279	4995.8	4.9958E5	3.411E-3	0.2	2.7
10.012	252.8	1946.8	10000	20.0	5.435	161.012	154.9	505.6	0.3064	8650	2709.4600	0.03384	5418.9	5.4189E5	3.411E-3	0.2	2.7
11.020	246.7	1878.5	10000	20.0	5.471	162.020	149.5	493.3	0.3030	8707	3016.2700	0.03578	6032.5	6.0325E5	3.411E-3	0.2	2.7
12.008	242.6	1804.9	10000	20.0	5.468	163.008	143.6	485.2	0.2960	8703	3219.8301	0.03697	6439.7	6.4397E5	3.411E-3	0.2	2.7
13.024	238.5	1775.2	10000	20.0	5.479	164.024	141.3	476.9	0.2962	8720	3416.8201	0.03833	6833.6	6.8336E5	3.411E-3	0.2	2.7
14.008	232.4	1705.2	10000	20.0	5.511	165.008	135.7	464.7	0.2920	8772	3704.6101	0.04061	7409.2	7.4092E5	3.411E-3	0.2	2.8
15.024	228.3	1631.0	10000	20.0	5.535	166.024	129.8	456.7	0.2842	8809	3893.2000	0.04224	7786.4	7.7864E5	3.411E-3	0.3	2.8
16.004	222.2	1555.5	10000	20.0	5.531	167.004	123.8	444.3	0.2786	8803	4174.6299	0.04459	8349.3	8.3493E5	3.411E-3	0.3	2.8
17.008	218.0	1520.3	10000	20.0	5.541	168.008	121.0	436.0	0.2775	8819	4357.8901	0.04640	8715.8	8.7158E5	3.411E-3	0.3	2.8
18.004	211.9	1447.5	10000	20.0	5.564	169.004	115.2	423.9	0.2718	8856	4619.0098	0.04930	9238.0	9.2380E5	3.411E-3	0.3	2.8
19.008	207.8	1408.8	10000	20.0	5.563	170.008	112.1	415.6	0.2698	8854	4793.2598	0.05126	9586.5	9.5865E5	3.411E-3	0.3	2.8
20.012	203.6	1355.0	10000	20.0	5.572	171.012	107.8	407.2	0.2648	8868	4968.3599	0.05349	9936.7	9.9367E5	3.411E-3	0.3	2.9
21.008	197.5	1288.3	10000	20.0	5.610	172.008	102.5	395.0	0.2596	8929	5212.1201	0.05724	10424	1.0424E6	3.411E-3	0.4	2.9
22.020	193.4	1238.4	10000	20.0	5.614	173.020	98.55	386.8	0.2548	8935	5374.7202	0.05973	10749	1.0749E6	3.411E-3	0.4	2.9
23.024	187.1	1171.6	10000	20.0	5.629	174.024	93.24	374.2	0.2491	8959	5612.3198	0.06397	11225	1.1225E6	3.411E-3	0.4	2.9
24.004	183.1	1124.5	10000	20.0	5.638	175.004	89.48	366.2	0.2443	8972	5762.1899	0.06690	11524	1.1524E6	3.411E-3	0.4	2.9
25.020	179.0	1091.1	10000	20.0	5.652	176.020	86.83	358.0	0.2425	8995	5912.2100	0.07018	11824	1.1824E6	3.411E-3	0.4	2.9
26.008	172.7	1023.6	10000	20.0	5.665	177.008	81.45	345.3	0.2359	9016	6137.1699	0.07559	12274	1.2274E6	3.411E-3	0.4	3.0
27.004	168.6	984.04	10000	20.0	5.665	178.004	78.31	337.2	0.2322	9017	6274.6802	0.07931	12549	1.2549E6	3.411E-3	0.5	3.0
28.008	162.4	931.18	10000	20.0	5.681	179.008	74.10	324.8	0.2281	9041	6481.5898	0.08568	12963	1.2963E6	3.411E-3	0.5	3.0
29.004	158.2	887.86	10000	20.0	5.690	180.004	70.65	316.4	0.2233	9056	6618.2202	0.09048	13236	1.3236E6	3.411E-3	0.5	3.0
30.020	154.1	849.84	10000	20.0	5.697	181.020	67.63	308.2	0.2194	9067	6745.1299	0.09543	13490	1.3490E6	3.411E-3	0.5	3.0
31.016	148.0	801.96	10000	20.0	5.703	182.016	63.82	295.9	0.2157	9077	6931.2598	0.1037	13863	1.3863E6	3.411E-3	0.5	3.0
32.008	143.7	763.41	10000	20.0	5.718	183.008	60.75	287.5	0.2113	9101	7056.6899	0.1101	14113	1.4113E6	3.411E-3	0.5	3.1
33.004	139.5	723.48	10000	20.0	5.727	184.004	57.57	278.9	0.2064	9114	7178.1401	0.1171	14356	1.4356E6	3.411E-3	0.6	3.1
34.004	133.4	675.11	10000	20.0	5.737	185.004	53.72	266.7	0.2014	9131	7342.2700	0.1283	14685	1.4685E6	3.411E-3	0.6	3.1
35.020	129.1	634.21	10000	20.0	5.747	186.020	50.47	258.3	0.1954	9146	7455.1299	0.1371	14910	1.4910E6	3.411E-3	0.6	3.1
36.004	124.7	603.09	10000	20.0	5.756	187.004	47.99	249.5	0.1924	9161	7568.8599	0.1472	15138	1.5138E6	3.411E-3	0.6	3.1
37.008	118.5	562.40	10000	20.0	5.756	188.008	44.75	237.1	0.1888	9161	7717.0898	0.1630	15434	1.5434E6	3.411E-3	0.6	3.1
38.008	114.3	523.21	10000	20.0	5.765	189.008	41.64	228.6	0.1821	9176	7816.1499	0.1756	15632	1.5632E6	3.411E-3	0.6	3.2
39.020	109.9	488.81	10000	20.0	5.777	190.020	38.90	219.8	0.1770	9194	7959.6401	0.1903	15919	1.5919E6	3.411E-3	0.7	3.2
40.012	103.7	446.70	10000	20.0	5.786	191.012	35.55	207.4	0.1714	9209	8047.2202	0.2141	16094	1.6094E6	3.411E-3	0.7	3.2
41.004	99.44	412.77	10000	20.0	5.793	192.004	32.85	198.9	0.1652	9220	8133.5200	0.2331	16267	1.6267E6	3.411E-3	0.7	3.2
42.012	95.00	393.49	10000	20.0	5.794	193.012	31.31	190.0	0.1648	9221	8220.9404	0.2554	16442	1.6442E6	3.411E-3	0.7	3.2
43.000	88.81	346.03	10000	20.0	5.804	194.000	27.54	177.6	0.1550	9238	8332.5996	0.2928	16665	1.6665E6	3.411E-3	0.7	3.2
44.004	84.55	320.70	10000	20.0	5.808	195.004	25.52	169.1	0.1509	9243	8407.4102	0.3233	16815	1.6815E6	3.411E-3	0.7	3.3
45.012	80.08	292.92	10000	20.0	5.815	196.012	23.31	160.2	0.1455	9255	8481.4004	0.3608	16963	1.6963E6	3.411E-3	0.8	3.3
46.004	73.48	253.22	10000	20.0	5.820	197.004	20.15	147.0	0.1371	9262	8580.6504	0.4289	17161	1.7161E6	3.411E-3	0.8	3.3
47.020	69.18	230.49	10000	20.0	5.831	198.020	18.34	138.4	0.1326	9280	8642.5801	0.4848	17285	1.7285E6	3.411E-3	0.8	3.3
48.004	64.59	208.71	10000	20.0	5.833	199.004	16.61	129.2	0.1286	9283	8704.3496	0.5563	17409	1.7409E6	3.411E-3	0.8	3.3
49.004	59.93	181.21	10000	20.0	5.841	200.004	14.42	119.9	0.1203	9296	8759.8496	0.6469	17520	1.7520E6	3.411E-3	0.8	3.3
50.008	55.70	160.12	10000	20.0	5.844	201.008	12.74	111.4	0.1144	9301	8809.5498	0.7494	17619	1.7619E6	3.411E-3	0.8	3.4
51.008	51.13	144.25	10000	20.0	5.845	202.008	11.48	102.3	0.1123	9303	8884.9404	0.8898	17770	1.7770E6	3.411E-3	0.9	3.4
52.020	44.43	114.14	10000	20.0	5.850	203.020	9.083	88.86	0.1022	9311	8920.2402	1.179	17840	1.7840E6	3.411E-3	0.9	3.4
53.008	40.11	96.463	10000	20.0	5.852	204.008	7.676	80.23	0.09568	9314	8956.8604	1.447	17914	1.7914E6	3.411E-3	0.9	3.4
54.008	35.30	76.966	10000	20.0	5.859	205.008	6.125	70.61	0.08675	9325	8993.6602	1.870	17987	1.7987E6	3.411E-3	0.9	3.4
55.012	30.27	60.321	10000	20.0	5.862	206.012	4.800	60.54	0.07929	9330	9023.7998	2.546	18048	1.8048E6	3.411E-3	0.9	3.4
56.008	25.99	47.960	10000	20.0	5.862	207.008	3.816	51.97	0.07343	9329	9048.0703	3.454	18096	1.8096E6	3.411E-3	0.9	3.5
57.004	20.92	33.718	10000	20.0	5.866	208.004	2.683	41.84	0.06413	9336	9071.6699	5.333	18143	1.8143E6	3.411E-3	1.0	3.5
58.008	17.92	25.682	10000	20.0	5.865	209.008	2.044	35.84	0.05703	9334	9083.2598	7.268	18167	1.8167E6	3.411E-3	1.0	3.5
59.020	11.24	11.890	10000	20.0	5.870	210.020	0.9462	22.47	0.04211	9342	9100.0303	18.50	18200	1.8200E6	3.411E-3	1.0	3.5
60.020	5.698	2.8083	10000	20.0	5.871	211.020	0.2235	11.40	0.01961	9345	9107.9502	71.95	18216	1.8216E6	3.411E-3	1.0	3.5

